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  • General Chemistry II Laboratory

General Chemistry II Laboratory

Adrian Ramirez Pranav Veera Buffers Part B: 1-) Formic Acid and Sodium Formate (Target pH=3.74) log[A/B]=pH-pKa log[A/B] =3.74-3.74 [A/B]=0 A/B = 1 0.1M=[A]+[B] [A]=[B]=0.05M M1V1= M2V2 (0.50M) V1= (0.05)x(0.1) V1=0.01L= 10ml (of Formic Acid and Sodium Formate needed) 2-) Formic Acid and Sodium Formate (Target pH=4.04) log[A/B]=pH-pKa log[A/B]=3.74-4.04 [A]/[B]=10-0.3=0.501 [B]=(0.501) x[A] 0.1M=[A]+[B] 0.1M= [A]+(0.501) A 0.1M=1.501A A=0.067; B=0.033M M1V1=M2V2 (0.5M) V1= (0.067) (100) V1=13.4mL (0.5) V1= (0.033) (100ml) V1= 6.6mL Acetic acid and sodium acetate (target pH= 4.44 and 5.04) for buffer 3 and 4. Part C: Determination of buffer capacity Acid/Base Pair Formic acid/ Formic acid/ Acetic acid/ Acetic acid/ Sodium formate Sodium formate 0.005 0.0033 Sodium acetate 0.0067 Sodium acetate 0.0033 Mols of Acid in Buffer Target pH Initial pH Vol of NaOH Mol of NaOH 3.74 3.84 9.53 0.0368 4.04 3.7 4.7 0.00235 4.44 4.45 5.0 0.0025 5.04 5.05 1.8 0.0009 The sodium formate and formic acid; buffer 1 and 2, the initial pH was not very close to the target pH. Buffer 1 initial pH has a margin of error of 10%; while buffer 2 has a margin of error of almost 34%. In contrast, in buffer of acetic acid and sodium acetate the initial pH was almost the target pH; with a margin of error of about 1%. Some possible causes of this elevated percentage of error may be due to measurement and observational errors; also, it could be due to contamination or environmental influences. In order to reach buffer capacity, we added between 0.0009 and 0.0368 mol of NaOH, this is because NaOH is a strong base thus it will react with the acid present in the buffer. I can conclude that Acetic acid/ Sodium acetate has a greater buffer capacity because it took most of the excess base taking the initial pH closer to the target pH. References: 1-https://www.voutube.com/watch?v=HzFIdpThd-s 2-The Properties of Buffer Handou