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Organic Chemistry

Paula Yurkanis Bruice

Chapter 7

The Reactions of Alkynes • An Introduction to Multistep Synthesis - all with Video Answers

Educators


Chapter Questions

01:32

Problem 1

Name the following:
a. $\operatorname{Br} \mathrm{CH}_{2} \mathrm{CH}_{2} \mathrm{C} \equiv \mathrm{CCH}_{3}$
b.
c. $\mathrm{CH}_{3} \mathrm{OCH}_{2} \mathrm{C} \equiv \mathrm{CCH}_{2} \mathrm{CH}_{3}$
d.

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01:57

Problem 2

Name the following:

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02:16

Problem 3

What is the molecular formula for a monocyclic hydrocarbon with 14 carbons and 2 triple bonds?

Madeline Currie
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04:55

Problem 4

Draw the condensed and skeletal structures for each of the following:
a. 1 -chloro- 3 -hexyne
b. cyclooctyne
c. isopropylacetylene
d. sec-butylisobutylacetylene
e. 4,4 -dimethyl-1-pentyne
f. dimethylacetylene

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05:21

Problem 5

Draw the structures and give the common and systematic names for the seven alkynes with molecular formula $\mathrm{C}_{6} \mathrm{H}_{10}$.

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04:49

Problem 6

Name the following:
a. $\mathrm{CH}_{2}=\mathrm{CHCH}_{2} \mathrm{C} \equiv \mathrm{CCH}_{2} \mathrm{CH}_{3}$
b.
c.
d. $\mathrm{HOCH}_{2} \mathrm{CH}_{2} \mathrm{C} \equiv \mathrm{CH}$
e. $\mathrm{CH}_{3} \mathrm{CH}=\mathrm{CHCH}=\mathrm{CHCH}=\mathrm{CH}_{2}$
f.

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02:16

Problem 7

Name the following:

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03:53

Problem 8

What orbitals are used to form the carbon-carbon $\sigma$ bond between the highlighted carbons?
a. $\mathrm{CH}_{3} \mathrm{CH}=\mathrm{CHCH}_{3}$
b. $\mathrm{CH}_{3} \mathrm{CH}=\mathrm{CHCH}_{3}$
c. $\mathrm{CH}_{3} \mathrm{CH}=\mathrm{C}=\mathrm{CH}_{2}$
d. $\mathrm{CH}_{3} \mathrm{C} \equiv \mathrm{CCH}_{3}$
e. $\mathrm{CH}_{3} \mathrm{C} \equiv \mathrm{CCH}_{3}$
f. $\mathrm{CH}_{2}=\mathrm{CHCH}=\mathrm{CH}_{2}$
g. $\mathrm{CH}_{3} \mathrm{CH}=\mathrm{CHCH}_{2} \mathrm{CH}_{3}$
h. $\mathrm{CH}_{3} \mathrm{C} \equiv \mathrm{CCH}_{2} \mathrm{CH}_{3}$
i. $\mathrm{CH}_{2}=\mathrm{CHC} \equiv \mathrm{CH}$

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01:30

Problem 9

In Table $7.2,$ what is the smallest alkane, the smallest terminal alkene, and the smallest terminal alkyne that are liquids at room temperature, which is generally taken to be $20^{\circ} \mathrm{C}$ to $25^{\circ} \mathrm{C} ?$

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01:14

Problem 10

Why does cis-2-butene have a higher boiling point than trans-2-butene?

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02:29

Problem 11

Under what circumstances can you assume that the less stable of two compounds is the more reactive compound?

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04:12

Problem 12

What is the major product of each of the following reactions?
a. $\mathrm{HC} \equiv \mathrm{CCH}_{3} \quad \stackrel{\mathrm{HBr}}{\longrightarrow}$
b.
c.
d.
e.
f.

Madeline Currie
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02:28

Problem 13

Drawing on what you know about the stereochemistry of alkene addition reactions,
a. write the mechanism for the reaction of 2 -butyne with one equivalent of $\mathrm{Br}_{2}$.
b. predict the configuration of the product of the reaction.

Madeline Currie
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02:42

Problem 14

What ketones are formed from the acid-catalyzed hydration of 3 -heptyne?

Madeline Currie
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01:54

Problem 15

Which alkyne should be used for the synthesis of each of the following ketones?

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01:49

Problem 16

Draw all the enol tautomers for each of the ketones in Problem 15.

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03:10

Problem 17

For each of the following alkynes, draw the products obtained from (1) the acid-catalyzed addition of water (mercuric ion is added for part a) and from (2) hydroboration-oxidation:
a. 1 -butyne
b. 2-butyne
c. 2 -pentyne

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00:58

Problem 18

Only one alkyne forms an aldehyde when it undergoes the mercuric-ion-catalyzed addition of water. Identify the alkyne.

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02:19

Problem 19

Describe the alkyne you should start with and the reagents you should use if you want to synthesize
a. pentane.
b. cis-2-butene.
c. trans-2-pentene.
d. 1 -hexene.

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02:43

Problem 20

What are products of the following reactions?

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01:55

Problem 21

Which of the following bases can remove a proton from a terminal alkyne in a reaction that favors products?
$$\mathrm{CH}_{3} \mathrm{O}^{-} \quad \mathrm{NH}_{3} \quad \mathrm{CH}_{3} \overline{\mathrm{C}} \mathrm{H}_{2} \quad \mathrm{H}_{2} \mathrm{C}=\overline{\mathrm{C}} \mathrm{H} \quad \mathrm{F}^{-}$$

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02:03

Problem 22

Explain why an amide ion cannot be used to form a carbanion from an alkane in a reaction that favors products.

Madeline Currie
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01:25

Problem 23

Any base whose conjugate acid has a $\mathrm{p} K_{\mathrm{a}}$ greater than _____ can remove a proton from a terminal alkyne to form an acetylide ion (in a reaction that favors products).

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02:34

Problem 24

Rank the following from strongest base to weakest base:
a. $\mathrm{CH}_{3} \mathrm{CH}_{2} \mathrm{CH}=\overline{\mathrm{C}} \mathrm{H} \quad \mathrm{CH}_{3} \mathrm{CH}_{2} \mathrm{C} \equiv \overline{\mathrm{C}} \quad \mathrm{CH}_{3} \mathrm{CH}_{2} \mathrm{CH}_{2} \overline{\mathrm{C}} \mathrm{H}_{2}$
b. $\mathrm{CH}_{3} \mathrm{CH}_{2} \mathrm{O}^{-} \quad \mathrm{F}^{-} \quad \mathrm{CH}_{3} \mathrm{C} \equiv \mathrm{C}^{-} \quad ^{-}\mathrm{NH}_{2}$

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00:37

Problem 25

Which carbocation is more stable?
$$\mathrm{CH}_{3} \mathrm{CH}_{2} \text { or } \mathrm{H}_{2} \mathrm{C}=\mathrm{CH}$$

Madeline Currie
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00:52

Problem 26

Which carbocation is more stable?
a. $\mathrm{H}_{2} \mathrm{C}=\mathrm{CH} \quad$ or $\quad \mathrm{HC} \equiv \mathrm{C}^{+}$
b. $\mathrm{HC} \equiv \mathrm{C}^{+}$ or $\mathrm{CH}_{3}^{+} \mathrm{CH}_{2}$

Madeline Currie
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01:43

Problem 27

A chemist wants to synthesize 3 -heptyne but cannot find any 1 -pentyne, the starting material used in the synthesis just described. How else can 3-heptyne be synthesized?

Madeline Currie
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05:48

Problem 28

How could the following compounds be synthesized from acetylene?
a. $\mathrm{CH}_{3} \mathrm{CH}_{2} \mathrm{CH}_{2} \mathrm{C} \equiv \mathrm{CH}$
b.
c. $\mathrm{CH}_{3} \mathrm{CH}=\mathrm{CH}_{2}$
d.
e.
f.

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02:04

Problem 29

What is the major product obtained from the reaction of each of the following compounds with excess HCI?
a. $\mathrm{CH}_{3} \mathrm{CH}_{2} \mathrm{C} \equiv \mathrm{CH}$
b. $\mathrm{CH}_{3} \mathrm{CH}_{2} \mathrm{C} \equiv \mathrm{CCH}_{2} \mathrm{CH}_{3}$
c. $\mathrm{CH}_{3} \mathrm{CH}_{2} \mathrm{C} \equiv \mathrm{CCH}_{2} \mathrm{CH}_{2} \mathrm{CH}_{3}$

Madeline Currie
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04:20

Problem 30

Draw a condensed structure for each of the following:
a. 2 -hexyne
b. 5 -ethyl- 3 -octyne
c. methylacetylene
d. vinylacetylene
e. methoxyethyne
f. sec-butyl-tert-butylacetylene
g. 1 -bromo-l-pentyne
h. 5 -methyl- 2 -cyclohexenol
i. diethylacetylene
j. di-tert-butylacetylene
k. cyclopentylacetylene
l. 5,6 -dimethyl- 2 -heptyne

Madeline Currie
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02:32

Problem 31

A student was given the structural formulas of several compounds and was asked to give them systematic names. How many did she name correctly? Correct those that are misnamed.
a. 4 -ethyl- 2 -pentyne
b. 1 -bromo- 4 -heptyne
c. 2 -methyl- 3 -hexyne
d. 3 -pentyne

Madeline Currie
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01:53

Problem 32

Identify the electrophile and the nucleophile in each of the following reaction steps. Then draw curved arrows to illustrate the bond-making and bond-breaking processes.
- Each arrow represents the movement of two electrons from a nucleophile to an electrophile.
- The tail of the arrow is positioned where the electrons are in the reactant.
- The tail of the arrow always stars at a lone pair or a bond.
The head of the arrow points to where these electrons will end up.
- The head of the arrow always points at an atom or at a bond.

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03:16

Problem 33

What is each compound's systematic name?

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02:44

Problem 34

What reagents should be used to carry out the following syntheses?

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08:27

Problem 35

a. Draw the structures and give the common and systematic names for alkynes with molecular formula $\mathrm{C}_{7} \mathrm{H}_{12} .$ Ignore stereosiomers. (Hint: There are 14.)
b. How many would there be if stereoisomers are included?

Madeline Currie
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01:55

Problem 36

Draw the mechanism for the following reaction:

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03:26

Problem 37

How can the following compounds be synthesized, starting with a hydrocarbon that has the same number of carbons as the desired product?
a.
b. $\mathrm{CH}_{3} \mathrm{CH}_{2} \mathrm{CH}_{2} \mathrm{CH}_{2} \mathrm{OH}$
c.

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01:15

Problem 38

What reagents would you use for the following syntheses?
a. $(Z)-3$ -hexene from 3 -hexyne
b. $(E)-3$ -hexene from 3 -hexyne
c. hexane from 3 -hexyne

Madeline Currie
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04:15

Problem 39

What is the major product of the reaction of 1 mol of propyne with each of the following reagents?
a. HBr (1 mol)
b. HBr (2 mol)
c. $\mathrm{Br}_{2}(1 \mathrm{mol}) / \mathrm{CH}_{2} \mathrm{Cl}_{2}$
d. $\mathrm{Br}_{2}(2 \mathrm{mol}) / \mathrm{CH}_{2} \mathrm{Cl}_{2}$
e. aqueous $\mathrm{H}_{2} \mathrm{SO}_{4}, \mathrm{HgSO}_{4}$
f. $\mathrm{R}_{2} \mathrm{BH}$ in $\mathrm{THF}$ followed by $\mathrm{H}_{2} \mathrm{O}_{2} / \mathrm{HO}^{-} / \mathrm{H}_{2} \mathrm{O}$
g. excess $\mathrm{H}_{2}, \mathrm{Pd} / \mathrm{C}$
h. $\mathrm{H}_{2} /$ Lindlar catalyst
i. sodium amide
j. the product of part i followed by 1-chloropropane

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03:01

Problem 40

Answer Problem 37 , parts a-h using 2 -butyne as the starting material instead of propyne.
What will be the major product of the reaction of 1 mol of propyne with each of the following reagents?
a. HBr (1 mol)
b. HBr (2 mol)
c. Br $2(1 \mathrm{mol}) / \mathrm{CH} 2 \mathrm{Cl} 2$
d. Br $2(2 \mathrm{mol}) / \mathrm{CH} 2 \mathrm{C} 12$
e. aqueous $\mathrm{H} 2 \mathrm{SO} 4, \mathrm{HgSO}$
f. $\mathrm{R} 2 \mathrm{BH}$ in THF followed by $\mathrm{H} 2 \mathrm{O} 2 / \mathrm{HO}-/ \mathrm{H} 2 \mathrm{O}$
g. excess $\mathrm{H} 2, \mathrm{Pd} / \mathrm{C}$
h. H2/Lindlar catalyst
i. sodium amide
J. the product of part i followed by 1 -chloropropane

Madeline Currie
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03:39

Problem 41

What is each compound's systematic name?
a. $\mathrm{CH}_{3} \mathrm{C}=\mathrm{CCH}_{2} \mathrm{CH}_{2} \mathrm{CH}_{2} \mathrm{CH}=\mathrm{CH}_{2}$
b.
c. $\mathrm{CH}_{3} \mathrm{CH}_{2} \mathrm{C} \equiv \mathrm{CCH}_{2} \mathrm{CH}_{2} \mathrm{C} \equiv \mathrm{CH}$
d.
e.
f.

Madeline Currie
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01:41

Problem 42

What is the molecular formula of a hydrocarbon that has 1 triple bond, 2 double bonds, 1 ring, and 32 carbons?

Nicole Krahulik
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04:18

Problem 43

a. Starting with 3-methyl-1-butyne, how can you prepare the following alcohols?
1. 2-methyl-2-butanol
2. 3-methyl-1-butanol
b. In each case, a second alcohol would also be obtained. What alcohol would it be?

Madeline Currie
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03:31

Problem 44

Which of the following names are correct? Correct those that are not correct.
a. 4 -heptyne
b. 2 -ethyl- 3 -hexyne
c. 4 -chloro- 2 -pentyne
d. 2,3 -dimethyl- 5 -octyne
e. 4,4 -dimethyl- 2 -pentyne
f. 2,5 -dimethyl- 3 -hexyne

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01:37

Problem 45

Which of the following pairs are keto-enol tautomers?

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05:30

Problem 46

How can the following compounds be prepared using ethyne as the starting material?

Madeline Currie
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01:47

Problem 47

Do the equilibria of the following acid-base reactions lie to the right or the left? (The $\left.\mathrm{p} K_{\mathrm{a}} \text { of } \mathrm{H}_{2} \mathrm{O}_{2} \text { is } 11.6 .\right)$
$$\begin{aligned}\mathrm{HOOH}+\mathrm{HO}^{-} & \rightleftharpoons \mathrm{HOO}^{-}+\mathrm{H}_{2} \mathrm{O} \\ \mathrm{RC} \equiv \mathrm{CH}+\mathrm{HOO}^{-} & \rightleftharpoons \mathrm{RC} \equiv \mathrm{C}^{-}+\mathrm{HOOH} \end{aligned}$$

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04:33

Problem 48

What is each compound's systematic name?

Madeline Currie
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03:54

Problem 49

What stereoisomers are obtained when 2 -butyne undergoes each of the following reaction sequences?
a. $1 . \mathrm{H}_{2} /$ Lindlar catalyst $2 . \mathrm{Br}_{2} / \mathrm{CH}_{2} \mathrm{Cl}_{2}$
b. $1 . \mathrm{Na} / \mathrm{NH}_{3}(\mathrm{liq}),-78^{\circ} \mathrm{C} 2 . \mathrm{Br}_{2} / \mathrm{CH}_{2} \mathrm{Cl}_{2}$
c. $1 . \mathrm{Cl}_{2} / \mathrm{CH}_{2} \mathrm{Cl}_{2}$ 2. $\mathrm{Br}_{2} / \mathrm{CH}_{2} \mathrm{Cl}_{2}$

Madeline Currie
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02:22

Problem 50

Show how the following compounds can be synthesized starting with ethyne:
a. cis- 2 -octene
b. trans-3-heptene

Madeline Currie
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01:07

Problem 51

Draw the keto tautomer for each of the following:

Madeline Currie
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05:31

Problem 52

Show how each of the following compounds can be prepared using the given starting material, any needed inorganic reagents, and any organic compound that has no more than four carbons:

Madeline Currie
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01:31

Problem 53

A chemist is planning to synthesize 3 -octyne by adding 1 -bromobutane to the product obtained from the reaction of 1-butyne with sodium amide. Unfortunately, however, he forgot to order 1-butyne. How else can he prepare 3-octyne?

Madeline Currie
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01:54

Problem 54

a. Explain why a single pure product is obtained from hydroboration-oxidation of 2 -butyne, whereas two products are obtained from hydroborationoxidation of 2 -pentyne.
b. Name two other internal alkynes that yield only one product upon hydroboration-oxidation.

Madeline Currie
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02:05

Problem 55

What stereoisomers are obtained from the following reactions?
a. $\mathrm{CH}_{3} \mathrm{CH}_{2} \mathrm{C} \equiv \mathrm{CCH}_{2} \mathrm{CH}_{3}$
1. $\mathrm{Na}, \mathrm{NH}_{3}(\text { liq }),-78^{\circ} \mathrm{C}$
2. $\mathrm{D}_{2}, \mathrm{Pd} / \mathrm{C}$
b. $\mathrm{CH}_{3} \mathrm{CH}_{2} \mathrm{C} \equiv \mathrm{CCH}_{2} \mathrm{CH}_{3}$
1. $\mathrm{H}_{2} /$ Lindlar catalyst
2. $\mathrm{D}_{2}, \mathrm{Pd} / \mathrm{C}$

Madeline Currie
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01:25

Problem 56

Explain why, in hydroboration-oxidation, $\mathrm{HO}^{-}$ and $\mathrm{HOOH}$ cannot be added until after the hydroboration reaction is over.

Madeline Currie
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05:38

Problem 57

Starting with ethyne, describe how the following compounds can be synthesized:
a. $(3 S, 4 R)$-4-bromo-3-hexanol and $(3 R, 4 S)$-4-bromo-3-hexanol
b. $(3 R, 4 R)$-4-bromo-3-hexanol and $(3 S, 4 S)$-4-bromo-3-hexanol

Madeline Currie
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02:27

Problem 58

$\alpha$ -Farnesene is a dodecatetraene found in the waxy coating of apple skins. What is its systematic name? Include $E$ and $Z$ where necessary to indicate the configuration of the double bonds.

Madeline Currie
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02:24

Problem 59

Show how the following compound can be prepared from the given starting material. Draw the structure of the compound that is formed in each step of the synthesis.

Madeline Currie
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04:15

Problem 60

What are the products of the following reactions?

Madeline Currie
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